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Electrochemical effects related to synthesis in micro reactors operating under electrokinetic flow [An article from: Chemical Engineering Journal]
Description
This digital document is a journal article from Chemical Engineering Journal, published by Elsevier in 2004. The article is delivered in HTML format and is available in your Amazon.com Media Library immediately after purchase. You can view it with any web browser.
Description:
We have demonstrated that peptides may be prepared in quantitative conversion in a micro reactor by reaction of the pentafluorophenyl (PFP) ester derivatives of protected amino acids. It was found that performing these reactions in a micro reactor operating under electrokinetic control resulted in an increase in reaction efficiency compared with the traditional batch method. By addition of an electrode to batch reactions, we propose that the enhancement in reaction rate is due to an electrochemical effect.
Description:
We have demonstrated that peptides may be prepared in quantitative conversion in a micro reactor by reaction of the pentafluorophenyl (PFP) ester derivatives of protected amino acids. It was found that performing these reactions in a micro reactor operating under electrokinetic control resulted in an increase in reaction efficiency compared with the traditional batch method. By addition of an electrode to batch reactions, we propose that the enhancement in reaction rate is due to an electrochemical effect.
